Wednesday, April 17, 2013

Seeking CLARITY? Make it invisible for best results…


Biology has long sought a window into the human mind and with new technologies, today, it is possible to literally see through the brain!

In a recent report in the journal Nature, the authors have developed a new technology, called CLARITY, that render big chunks of tissue optically clear and permissive to immunolabeling.

Understanding the functioning of the brain and its transformation into the mind is one of the single biggest challenges facing biology today. And although work over the past few decades has given us a fairly good understanding of the brain at a microscopic level; we have lost out on the bigger picture that emerges from the interactions among the different microscopic areas – largely due to technological limitations (and the diffraction limit of light).  

Our current view of the brain is almost like a map of the world before the satellite technology came in – remember the pre-google map/ pre-GPS era? Our reconstructions of the brain either involve microscopic examination of many smaller pieces aimed at re-creating the bigger picture or a gross overview of the bigger areas without the finer details. Not only does this piece-meal effort yield a partial and incomplete picture, it is labor intensive, expensive and time consuming. Also most of these techniques are often incompatible with molecular phenotyping of the intact tissue such that we most often get a crude map without any labels or orientation. This makes it virtually impossible to understand the landscape of the human brain. And mapping a place is truly critical to visiting and understanding it!

One possible solution to these technical challenges would be to render the intact tissue transparent to light and permeable to our molecular tags in their native location. Now, this sounds like the perfect dream but Prof. Karl Deisseroth and his team at the Stanford have achieved exactly this with their technology called CLARITY.

They figured that lipid bilayers or the cell membranes are the single biggest obstacle in making a tissue inaccessible to light (and hence imaging) and to our molecular probes; and if they could be selectively removed without destroying the structure and localization of the tissue, then we could get an optically clear 3-dimensional tissues that can be imaged with ease. But these cell membranes are what provide structure and integrity to the cells; without them we would be staring at a broth of many proteins and nucleic acids with no structure or localization. Thus, even as the lipid bilayers are removed, one needs to replace that framework with an alternative scaffold that can physically support the tissue and this is what they have achieved with their technology.

Briefly, they first immobilize the proteins and nucleic acids in the brain tissue by fixing them and crosslinking them with formaldehye and a hydrogel (acrylamide and bisacrylamide) that is liquid at low temperatures (and hence perfuses all through the tissue), but solidifies at higher temperatures. Formaldehyde is a strong, pungent smelling chemical that uses the amine groups (NH2 or nitrogen groups) of proteins and nucleic acids and crosslinks them to each other. This locks the cells and tissues in a state of complete inaction enabling additional manipulation (sectioning, staining, storing). While formaldehyde is routinely used in the hospitals and laboratories to store and “fix” tissue samples, it would not preserve structural integrity in the absence of lipid bilayers. Once the tissue is embalmed with this mix of a hydrogel and a fixative, the authors can now move the tissue to higher temperatures (37C) where the hydrogel will solidify and form a firm scaffold with the proteins and nucleic acids anchored on it.

At this point, the tissue is ready to be cleared off the lipids. And although using organic solvents like alcohol, benzene etc. would probably be an easier route to remove the lipid bilayers, this treatment usually quenches any fluorescence that the tissue may carry due to the expression of genetically encoded fluorescent proteins (like GFP, YFP, RFP etc.). To circumvent this problem, the authors used ionic detergents to remove the lipid layers, much like what your soap does. However, instead of relying on a slow (month-long) passive diffusion process, the authors applied an electric charge on the tissue to strip off the lipids along with the detergent. Since the proteins and the nucleic acids (also charged) were already cross-linked to the hydrogel, a small electric field should selectively strip out the lipids thus leaving behind an optically clear scaffolding of the brain with the proteins and nucleic acids anchored in place.

Using CLARITY, or Clear Lipid-exchanged Acrylamide-Hybridized Rigid Imaging/immunostaining/in situ hybridization compatible- Tissue hYdrogel, the authors managed to transform a mouse brain in 8 days into an optically clear, lipid-free, structurally stable hydrogel tissue hybrid. This tissue hybrid (map) could then be labeled for specific areas by the use of specific molecular probes (nucleic acid probes in FISH or antibodies against proteins) and imaged as a whole with standard microscopy that is routinely used.




Intact adult mouse brain Imaging before and after CLARITY.




CLARITY: Tissue is crosslinked with formaldehyde (red) in the presence of hydrogel monomers (blue), covalently linking tissue elements to monomers that are then polymerized into a hydrogel mess (followed by a 4 day wash step). Electric fields applied across the sample in ionic detergent actively transport micelles into, and lipids out of, the tissue, leaving fine-structured and cross-linked biomolecules in places. The ETC chamber for the electrophoresis is depicted in the boxed region.




Imaging was performed from an intact adult mouse brain using CLARITY. This is a non-sectioned mouse bran showing the cortex, hippocampus and thalamus (X10 objective; stack size 3400 uM; step size, 2uM).



Clearing tissues has been attempted for a long time now and for many end purposes like imaging, generating tissue scaffolds, developing tissue niches and synthetic organs. However, these approaches have relied on harsher methods that stripped the tissues off all biomolecules – lipids, nucleic acids and proteins – thus making the cleared tissue stripped of biological landmarks/ markers. Previous methods used detergents like SDS, urea, Triton X 100 and chemicals like Scale to strip the lipids from the tissue matrix and most of these methods also caused massive protein loss ranging anywhere between 65% to 25%.

With their improvements and modifications, CLARITY has enabled optical clearing of bigger and denser tissues with only 8% loss of the tissue protein thus allowing more landmarks in our map. The authors also found that replacing the impervious lipid bilayers with the porous hydrogel enabled the diffusion of the molecular probes deeper into the tissue – enabling greater access and better coverage.

Remarkably, these hybrid tissue scaffolds were also compatible to banked specimens that were fixed years ago with only formaldehyde. This further broadens the scope and utility of the technique as it makes available for study tissue samples banked and collected years before.

Although further improvements in imaging and computational techniques would enable a more refined, high throughput analysis, the use of CLARITY has certainly enabled integrative visualization of large scale biological systems. And within a few years, we might be able to have an accurate and labeled (satellite level) map of the landscape of a mammalian brain.

References:

2)   http://www.nature.com/news/see-through-brains-clarify-connections-1.12768

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